1.3 mm probe X/Y/H-F H13863
Probe description: PH MASDVT 850W6 BL1.3 X/Y/H-F
Maximum spinning speed 65kHz
Additional components: shunt capacitor 220pF; shunt capacitor 180pF
x/y combination | X f/MHz | Y f/MHz | Modification mode | Description insert |
Part no: |
29Si/15N-2H | 168.9 | 86-130.5 | λ/4 | 5 turns+ 1turn 12pF+3.3pF |
HZ16604 |
13C/15N-2H | 213.7 | 86 - 130.5 | λ/4 |
4 turns+1 turn |
HZ15355 |
23Na/15N-2H | 224.8 | 86 -130.5 | λ/4 | 5 turns+ 1turn 6.8pF+3.3pF |
HZ16606 |
23Na/29Si | 224.8 | 168.9 | λ/2 | 5 turns+ 1turn 6.8pF+3.3pF |
HZ16606 |
23Na/14N | 224.8 | 61.4 | with 220pF shunt and λ/4 | 5 turns+ 1turn 6.8pF+3.3pF |
HZ16606 |
27Al/14N-29Si | 221.5 | 61.4-168.9 | the same modifications as 23Na with 180pF for 14N |
5 turns+ 1turn 6.8pF+3.3pF |
HZ16605 |
11B/17O-29Si | 272.7 | 115.2-168.9 | λ/2 | 6 turns+ 1turn 3.3pF+3.3pF |
HZ16607 |
Probe Test Results (Stated 90o pulse lengths are the best achieved during installation. To reduce risk of damage to the probes, facility users should use slightly lower RF nutation frequencies (i.e. longer 90o pulse lengths) were possible. Please discuss with the facility manager appropriate RF nutation frequencies for your experiments.)
insert 29Si/15N-2H:
Nuc | 90opulse |
Pulse power |
Pulse power (W) |
Configuration 29Si/15N-2H |
Sample | Remarks |
29Si | 1.7 | 1 | 213 | λ/4 | Si-grease | |
15N | 2 | -1 | 442 | λ/4 | Glycine (CP) | S/N=5 (for 16 scans) |
1H | 1.23 | 4 | 71 | λ/4 | Glycine | acquisition time tested 45ms |
insert 13C/15N-2H:
Nuc | 90opulse |
Pulse power |
Pulse power (W) |
Configuration 13C/15N-2H |
Sample | Remarks |
79Br | 1.5 | 3.3 | 136 | λ/4 | KBr | |
13C | 1.5 | 3.3 | 142 | λ/4 | Adamantane | line width 1.6Hz |
1H | 1 | 1.6 | 123 | λ/4 | Adamantane | there is a 1H background visible |
13C | 2 | 5 | 96 | λ/4 | Glycine (CP) | S/N 42 (for 16 scans) |
1H | 1.23 | 3.6 | 78 | λ/4 | Glycine | 100kHz for 50ms decoupling |
15N | 3.45 | -2 | 556 | λ/4 | Glycine (CP) (enriched) | |
19F | 0.8 | 0 | 187 | λ/4 for 19F | pvdf | |
19F | 1.15 | 7 | 50 | λ/4 for 19F | pvdf | there is a 19F background visible |
13C | 1.8 | 4 | 121 | λ/4 for 19F | pvdf (19F CP) |
insert 23Na/15N-29Si:
Nuc | 90opulse |
Pulse power |
Pulse power (W) |
Configuration 23Na/15N-29Si |
Sample | Remarks |
23Na | 1.43 | 2 | 185 | λ/4 | NaCl | |
15N | 2 | -1 | 442 | λ/4 | Glycine (CP) | |
1H | 1.23 | 4 | 71 | λ/4 | Glycine | |
14N | 2.3 | 0 | 398 | λ/4 | NH4Cl |
insert 27Al/15N-29Si:
Nuc | 90opulse |
Pulse power |
Pulse power (W) |
Configuration 27Al/15N-29Si |
Sample | Remarks |
27Al | 1.6 | 2 | 156 | λ/4 | Al2NO3 | |
15N | 2 | -1 | 442 | λ/4 | Glycine (CP) | |
1H | 1.23 | 4 | 71 | λ/4 | Glycine |
insert 11B/29Si-17O:
Nuc | 90opulse |
Pulse power |
Pulse power (W) |
Configuration 11B/29Si-17O |
Sample | Remarks |
11B | 1.15 | 3.3 | 116 | λ/2 | Borax | |
2H | 2.3 | 0 | 232 | λ/2 | D2O |
DR mode:
Nuc | 90opulse |
Pulse power |
Pulse power (W) |
Configuration |
Sample | Remarks |
13C | 1.2 | 3.3 | 136 | λ/2 | Adamantane | line width 1.2Hz |
1H | .95 | 1.6 | 123 | λ/2 | Adamantane | |
13C | 1.6 | 5 | 96 | λ/2 | Glycine (CP) | S/N 53 (16 scans) |
1H | 1.27 | 3.8 | 74 | λ/2 | Glycine | |
19F | 0.82 | 4.3 | 93 | λ/4 | pvdf | |
13C | 1.25 | 3.3 | 136 | λ/4 | pvdf |
Tuning ranges (tested on the bench; probe in double-resonance mode 1H-X)
λ /4 mode |
61 →132 MHz |
Includes: 14N(61.424), 33S(65.246), 189Os(66.006), 21Ne(67.102), 176Lu(69.114), 37Cl(69.324), 131Xe(70.073), 169Tm(70.465), 61Ni(75.956), 91Zr(79.019), 85Rb( 82.067), 35Cl (83.282), 135Ba( 84.443), 50V( 84.748), 15N( 86.163), 10B(91.321), 153Eu(93.330), 137Ba( 94.460), 175Lu( 96.934), 181Ta(101.912), 123Sb( 110.153), 133Cs(111.487), 138La(112.152), 17O(115.230), 9Be( 119.440), 139La(120.068), 6Li(125.087), 2H(130.480) |
λ/2 mode |
150 → 215 MHz |
Includes: 77Se(162.108), 29Si(168.871), 127I(170.064), 207Pb( 177.825), 111Cd(180.332), 165Ho(181.390), 195Pt(182.723), 113In(185.859), 115In(186.257), 113Cd(188.642), 99Tc(191.321), 185Re(191.459), 187Re(193.389), 59Co(201.680), 121Sb(203.410), 69Ga(204.012), 159Tb(204.340), 45Sc(206.480), 93Nb(208.047), 55Mn(210.708), 151Eu(211.310), 79Br(212.959), 13C(213.733) |
λ/2 mode + range coil |
220 → 280 MHz |
27Al (221.483), 123Te(222.443), 51V(223.575), 23Na(224.841), 63Cu(225.382), 81Br(229.555), 129Xe(236.387), 65Cu(241.431), 71Ga(259.222), 141Pr(260.270), 125Te(268.173), 11B(272.714), 115Sn(278.109), 87Rb(278.124), 117Sn(302.874), 119Sn(316.970), 7Li(330.342), 31P(344.086) |