2.5 mm HX (+19F) H13889

Probe description: PH MASDVT850W6 BL2.5 14N-31P/F-H

Additional components: range coil (for ³¹P) (4 turns)

Probe Test Results (Stated 90^o pulse lengths are the best achieved during installation. To reduce risk of damage to the probes, facility users should use slightly lower RF nutation frequencies (i.e. longer 90^o pulse lengths) were possible. Please discuss with the facility manager appropriate RF nutation frequencies for your experiments.):

Nuc	90^opulse	Pulse power level (db)	Pulse power (W)	Configuration	Sample	Remarks
⁷⁹Br	2.0	2.2	176	λ/2	KBr
¹³C	2	2	192	λ/2	Adaman.	line width 1.6Hz
¹H	1.65	-1	225	λ/2	Adaman.	there is a visible ¹H background signal
¹³C	2.26	3.6	133	λ/2	Glycine (CP)	S/N 69 (4 scans)
¹H	1.7	0	113	λ/2	Glycine	147kHz for 50ms decoupling
¹⁵N	4	2.1	216	λ/4	Glycine (CP) (enriched)
¹⁵N	3.28	0	351	λ/4	Glycine (CP90) (enriched)
¹⁴N	2.75	-1	568	λ/4	NH4Cl
¹⁹F	1.8	0.4	171	λ/2	pvdf
³¹P	1.8	3	210	λ/2+range coil	ADP

Tuning range ¹H/X mode (measured on bench)

λ/2 mode

213 →344 MHz

Over 250MHz a range coil must be inserted

Includes: ¹³C(213.733), ²⁷Al (221.483), ¹²³Te(222.443), ⁵¹V(223.575), ²³Na(224.841), ⁶³Cu(225.382), ⁸¹Br(229.555), ¹²⁹Xe(236.387), ⁶⁵Cu(241.431), ⁷¹Ga(259.222), ¹⁴¹Pr(260.270), ¹²⁵Te(268.173), ¹¹B(272.714), ¹¹⁵Sn(278.109), ⁸⁷Rb(278.124), ¹¹⁷Sn(302.874), ¹¹⁹Sn(316.970), ⁷Li(330.342), ³¹P(344.086)

λ/4 mode

61 →168 MHz

¹⁷⁶Lu(69.114), ³⁷Cl (69.324), ¹³¹Xe(70.073), ¹⁶⁹Tm(70.465), ⁶¹Ni (75.956), ⁹¹Zr(79.019), ⁸⁵Rb( 82.067), ³⁵Cl (83.282), ¹³⁵Ba( 84.443), ⁵⁰V( 84.748), ¹⁵N( 86.163), ¹⁰B(91.321), ¹⁵³Eu( 93.330), ¹³⁷Ba( 94.460), ¹⁷⁵Lu( 96.934), ¹⁸¹Ta( 101.912), ¹²³Sb( 110.153), ¹³³Cs(111.487), ¹³⁸La( 112.152), ¹⁷O(115.230), ⁹Be( 119.440), ¹³⁹La(120.068), ⁶ Li(125.087), ²H(130.480), ²⁰⁹Bi(136.589), ⁷⁵As(145.542), ¹⁷¹Yb(148.744), ¹⁹⁹Hg(152.242), ⁷⁷Se(162.108), ²⁹Si(168.871)

Tuning range ¹⁹F/X mode (measured on bench)

λ/2 mode

213→344 MHz

Over 250MHz a range coil must be inserted