Probe description: PH MASDVT850W6 BL2.5 N-C/F/H

Operating intructions

Additional components: shunt capacitor 47pF

Frequency range:

15N-2H λ/4 mode with shunt capacitor	X MHz (ranges on bench)	19F/1H MHz (ranges on bench)
15N-2H/19F/1H	86-130	800/850

Frequency range:

29Si-13C λ/4 mode without shunt capacitor	X MHz (ranges on bench)	19F/1H MHz (ranges on bench)
29Si-13C/19F/1H	169-213	800/850

 

Probe Test Results (Stated 90^o pulse lengths are the best achieved during installation. To reduce risk of damage to the probes, facility users should use slightly lower RF nutation frequencies (i.e. longer 90^o pulse lengths) were possible. Please discuss with the facility manager appropriate RF nutation frequencies for your experiments.)

without shunt capacitor:

Nuc	90o pulse	Pulse power level (db)	Pulse power (W)	Configuration	Sample	Remarks
79Br	2.6	3.6	127	λ/4	KBr
13C	2.5	3.3	142	λ/4	Adaman.	line width 1.4Hz
1H	2.5	-.35	193	λ/4	Adaman.	there is a visible 1H background
19F	2.2	-0.8	301	λ/4	pvdf	background visible
1H	2.45	.3	167	λ/4	Glycine	147kHz for 50ms decoupling
13C	2.7	4	121	λ/4	Glycine (CP)	S/N 43 (ns=4)
1H	2.6	1.2	135	λ/4	pvdf (CP)	Double decoupling (cpf2f3) 80kHz/89kHz
13C	2.8	4	121	λ/4	pvdf (CP)
19F	2.53	0.2	239	λ/4	pvdf (CP)	Double decoupling (cpf2f3) 100kHz/100kHz

 

with shunt capacitor :

Nuc	90o pulse	Pulse power level (db)	Pulse power (W)	Configuration	Sample	Remarks
1H	2.8	1.2	135	λ/4	Glycine
15N	3.4	1	275	λ/4	Glycine (CP) (enriched)
19F	2.1	-0.8	301	λ/4	pvdf
19F	2.4	0.2	239	λ/4	pvdf