4 mm HX (low gamma) H13892

Probe description: PH MASDVT850W6 BL4 103Rh-13C/1H

Probe Test Results (Stated 90^o pulse lengths are the best achieved during installation. To reduce risk of damage to the probes, facility users should use slightly lower RF nutation frequencies (i.e. longer 90^o pulse lengths) were possible. Please discuss with the facility manager appropriate RF nutation frequencies for your experiments.)

VT calibration report Temperature calibration temperature- spinning calibration

Nuc	90^o pulse	Pulse power level (db)	Pulse power (W)	Configuration	Sample	Remarks
⁷⁹Br	2.75	0	293	λ/2	KBr
¹³C	3	0	305	λ/2	Adaman.	line width 1.9Hz
¹H	2.62	-0.2	187	λ/2	Adaman.
¹³C	2.9	1	242	λ/2	Glycine (CP)	S/N 166
¹H	2.8	0	179	λ/2	Glycine (CP)	89kHz for 40ms decoupling
¹⁵N	6.6	0	351	λ/4	Glycine (CP)	S/N 21
¹⁵N	4.4	-3.57	800	λ/4	Glycine (CP90)
¹⁴N	5	-4	900	λ/4	NH4Cl

Tuning ranges (on bench)

λ/2 mode	168→ 213 MHz	Includes: ²⁹Si(168.871), ¹²⁷I(170.064), ²⁰⁷Pb( 177.825), ¹¹¹Cd(180.332), ¹⁶⁵Ho(181.390), ¹⁹⁵Pt(182.723), ¹¹³In(185.859), ¹¹⁵In(186.257), ¹¹³Cd(188.642), ⁹⁹Tc(191.321), ¹⁸⁵Re(191.459), ¹⁸⁷Re(193.389), ⁵⁹Co(201.680), ¹²¹Sb(203.410), ⁶⁹Ga(204.012), ¹⁵⁹Tb(204.340), ⁴⁵Sc(206.480), ⁹³Nb(208.047), ⁵⁵Mn(210.708), ¹⁵¹Eu(211.310), ⁷⁹Br(212.959), ¹³C(213.733)
λ/4 mode	27 → 130 MHz	¹⁰³Rh(27.085), ⁵⁷Fe(27.521), ¹⁴⁵Nd(28.560), ¹⁶¹Dy(29.240), ¹⁴⁹Sm(29.240), ⁷³Ge(29.651), ⁸³Kr(32.705), ¹⁷⁷Hf(34.059), ¹⁵⁷Gd(34.255), ¹⁰⁷Ag(34.406), ¹⁸³W(35.414), ¹⁴⁷Sm(35.445), ⁸⁷Sr (36.837), ¹⁰⁵Pd(38.897), ⁹⁹Ru(39.144), ¹⁰⁹Ag(39.555), ³⁹K(39.664), ¹⁶³Dy(40.970), ¹⁷³Yb(40.978), ⁸⁹Y(41.652), ¹⁰¹Ru(43.872), ¹⁴³Nd(46.325), ⁴⁷Ti (47.919), ⁴⁹Ti(47.932), ⁵³Cr(48.046), ⁴⁰K(49.317), ²⁵Mg(52.034), ⁶⁷Zn(53.183), ⁹⁵Mo(55.394), ²⁰¹Hg(56.198), ⁹⁷Mo(56.556), ⁴³Ca(57.205), ¹⁴N(61.424), ³³S(65.246), ¹⁸⁹Os(66.006), ²¹Ne(67.102), ¹⁷⁶Lu(69.114), ³⁷Cl(69.324), ¹³¹Xe(70.073), ¹⁶⁹Tm(70.465), ⁶¹Ni(75.956), ⁹¹Zr(79.019), ⁸⁵Rb( 82.067), ³⁵Cl (83.282), ¹³⁵Ba( 84.443), ⁵⁰V( 84.748), ¹⁵N( 86.163), ¹⁰B(91.321), ¹⁵³Eu(93.330), ¹³⁷Ba( 94.460), ¹⁷⁵Lu( 96.934), ¹⁸¹Ta(101.912), ¹²³Sb( 110.153), ¹³³Cs(111.487), ¹³⁸La(112.152), ¹⁷O(115.230), ⁹Be( 119.440), ¹³⁹La(120.068), ⁶ Li(125.087), ²H(130.480)