Skip to main content

4 mm HX (low gamma) H13892

Probe description: PH MASDVT850W6 BL4 103Rh-13C/1H

Operating instructions

Probe Test Results (Stated 90o pulse lengths are the best achieved during installation. To reduce risk of damage to the probes, facility users should use slightly lower RF nutation frequencies (i.e. longer 90o pulse lengths) were possible. Please discuss with the facility manager appropriate RF nutation frequencies for your experiments.)

VT calibration report Temperature calibration temperature- spinning calibration

 

Nuc 90o pulse

Pulse power
level (db)

Pulse
power (W)
Configuration Sample Remarks
79Br 2.75 0 293 λ/2 KBr  
13C 3 0 305 λ/2 Adaman. line width 1.9Hz
1H 2.62 -0.2 187 λ/2 Adaman.  
13C 2.9 1 242 λ/2 Glycine (CP) S/N 166
1H 2.8 0 179 λ/2 Glycine (CP) 89kHz for 40ms decoupling
15N 6.6 0 351 λ/4 Glycine (CP) S/N 21
15N 4.4 -3.57 800 λ/4 Glycine (CP90)  
14N 5 -4 900 λ/4 NH4Cl  

 

Tuning ranges (on bench)

λ/2 mode

168→ 213 MHz

Includes: 29Si(168.871), 127I(170.064), 207Pb( 177.825), 111Cd(180.332), 165Ho(181.390), 195Pt(182.723), 113In(185.859), 115In(186.257), 113Cd(188.642), 99Tc(191.321), 185Re(191.459), 187Re(193.389), 59Co(201.680), 121Sb(203.410), 69Ga(204.012), 159Tb(204.340), 45Sc(206.480), 93Nb(208.047), 55Mn(210.708), 151Eu(211.310), 79Br(212.959), 13C(213.733)

λ/4 mode

27 → 130 MHz

103Rh(27.085), 57Fe(27.521), 145Nd(28.560), 161Dy(29.240), 149Sm(29.240), 73Ge(29.651), 83Kr(32.705), 177Hf(34.059), 157Gd(34.255), 107Ag(34.406), 183W(35.414), 147Sm(35.445), 87Sr (36.837), 105Pd(38.897), 99Ru(39.144), 109Ag(39.555), 39K(39.664), 163Dy(40.970), 173Yb(40.978), 89Y(41.652), 101Ru(43.872), 143Nd(46.325), 47Ti (47.919), 49Ti(47.932), 53Cr(48.046), 40K(49.317), 25Mg(52.034), 67Zn(53.183), 95Mo(55.394), 201Hg(56.198), 97Mo(56.556), 43Ca(57.205), 14N(61.424), 33S(65.246), 189Os(66.006), 21Ne(67.102), 176Lu(69.114), 37Cl(69.324), 131Xe(70.073), 169Tm(70.465), 61Ni(75.956), 91Zr(79.019), 85Rb( 82.067), 35Cl (83.282), 135Ba( 84.443), 50V( 84.748), 15N( 86.163), 10B(91.321), 153Eu(93.330), 137Ba( 94.460), 175Lu( 96.934), 181Ta(101.912), 123Sb( 110.153), 133Cs(111.487), 138La(112.152), 17O(115.230), 9Be( 119.440), 139La(120.068), 6 Li(125.087), 2H(130.480)