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3.2 mm HXY low E field H13900

Probe description: PH MASDVT 850W6 BL3.2 X/Y/H LLC

Operating instructions

Probe Test Results (Stated 90o pulse lengths are the best achieved during installation. To reduce risk of damage to the probes, facility users should use slightly lower RF nutation frequencies (i.e. longer 90o pulse lengths) were possible. Please discuss with the facility manager appropriate RF nutation frequencies for your experiments.)

 

Insert 13C/15N:

Nuc 90o pulse 

 Pulse power
level (db)

 Pulse
power (W)
Configuration
13C/15N
Sample Remarks
79Br 5.2 -.9 360 λ/4 KBr  
13C 5.6 -1.2 400 λ/4 Adamantane  line width 5.2Hz
1H 2.7 -2.24 300 λ/4 Adamantane  
13C 5.6 -1.2 400 λ/4 Glycine (CP) S/N 36 (ns=4)
1H 2.43 -2 283 λ/4 Glycine acq for 50ms decoupling
15N 9 -1.53 500 λ/4 Glycine  

 

DR mode

Nuc 90o pulse 

 Pulse power
level (db)

 Pulse
power (W)
Configuration
Sample Remarks
79Br 3.5 -0.9 360 λ/2 KBr  
1H 3.5 .7 152 λ/2 Adamantane  
13C 3.6 -1.2 402 λ/2 Adamantane  
13C 3.7 0 305 λ/2 Glycine (CP) S/N 61 (ns=4)
1H 2.42 -2 283 λ/2 Glycine (CP)  

 

Tuning range (measured on the bench, double resonnace mode 1H-X ) 

λ/2 mode

151.5→281 MHz

Includes: 199Hg(152.242), 77Se(162.108), 29Si(168.871), 127I(170.064), 207Pb(177.825), 111Cd( 180.332), 165Ho(181.390), 195Pt(182.723), 113In(185.859), 115In(186.257), 113Cd(188.642), 99Tc(191.321), 185Re(191.459), 187Re(193.389), 59Co(201.680), 121Sb(203.410), 69Ga(204.012), 159Tb(204.340), 45Sc(206.480), 93Nb(208.047), 55Mn(210.708), 151Eu(211.310), 79Br(212.959), 13C(213.733), 27Al(221.483), 123Te(222.443), 51V(223.575), 23Na(224.841), 63Cu(225.382), 81Br(229.555), 129Xe(236.387), 65Cu(241.431), 71Ga(259.222), 141Pr(260.270), 125Te(268.173), 11B(272.714), 115Sn(278.109), 87Rb(278.124)

λ/4 mode

55→217 MHz

Includes: 95Mo(55.394), 201Hg(56.198), 97Mo(56.556), 43Ca(57.205), 14N(61.424), 33S(65.246), 189Os(66.006), 21Ne(67.102), 176Lu(69.114), 37Cl (69.324), 131Xe(70.073), 169Tm(70.465), 61Ni (75.956), 91Zr(79.019), 85Rb( 82.067), 35Cl (83.282), 135Ba( 84.443), 50V( 84.748), 15N( 86.163), 10B(91.321), 153Eu( 93.330), 137Ba( 94.460), 175Lu(96.934), 181Ta( 101.912), 123Sb( 110.153), 133Cs(111.487), 138La(112.152), 17O(115.230), 9Be( 119.440), 139La(120.068), 6 Li(125.087), 2H(130.480), 209Bi(136.589), 75As(145.542), 171Yb(148.744), 199Hg(152.242), 77Se(162.108), 29Si(168.871), 127I(170.064), 207Pb( 177.825), 111Cd( 180.332), 165Ho(181.390), 195Pt(182.723), 113In(185.859), 115In(186.257), 113Cd(188.642), 99Tc(191.321), 185Re(191.459), 187Re(193.389), 59Co(201.680), 121Sb(203.410), 69Ga(204.012), 159Tb(204.340), 45Sc(206.480), 93Nb(208.047), 55Mn(210.708), 151Eu(211.310), 79Br(212.959), 13C(213.733),