Nucleus |
90 pulse |
Power |
15N |
6 us |
450 W |
79Br |
5.5 us |
300 W |
inserts
C1 |
1.5 - 52 pF X tunning |
L1 |
PH MAS coil trim coil 7 1N 7T |
L2 |
PH MAS coil HTB7 1N 3.5T MGO CPL |
L3 |
PHMAS rangecoil X D8 8W WB, here only 2.5 turns |
X channel |
Nucleus |
15N |
2H |
13C |
31P |
XL / MHz |
84 |
105 |
196 |
197 |
XH / MHz |
183 |
200 |
281 |
348 |
∆F / MHz
|
2.4 |
4.1 |
10.1 |
9.3 |
Q |
99 |
136 |
144 |
245 |
Insert |
22 pF |
10 pF |
Leer |
Leer + Rangecoil L3 |
Laser Intensity (A) |
Laser power (W) |
K79Br Chemical shift (ppm) |
Sample Temperature (oC) (Delta/0.025) |
1 |
0 |
0 |
0 |
2 |
0 |
0 |
0 |
3 |
0 |
0 |
0 |
4 |
0 |
0 |
0 |
5 |
0 |
0 |
0 |
6 |
3.5 |
-0.7 |
28 |
7 |
5.7 |
-1.8 |
72 |
8 |
8.1 |
-2.8 |
112 |
9 |
10.2 |
-3.8 |
152 |
10 |
12.5 |
-5 |
200 |
11 |
15.1 |
-6 |
240 |
12 |
17.3 |
-6.7 |
268 |
13 |
19.7 |
-7.9 |
316 |
14 |
21.9 |
-8.7 |
348 |
15 |
24.2 |
-9.5 |
380 |
0 |
0 |
0 |
0 |
5 |
0 |
0 |
0 |
6 |
3.5 |
-0.8 |
32 |
7 |
5.7 |
-1.7 |
68 |
8 |
7.9 |
-2.9 |
116 |
9 |
10.2 |
-3.9 |
156 |
10 |
12.5 |
-5 |
200 |
11 |
15 |
-5.1 |
204 |
12 |
17.5 |
-6.7 |
268 |
13 |
19.6 |
-7.6 |
304 |
14 |
22.2 |
-8.5 |
340 |
15 |
24.3 |
-9.3 |
372 |
16 |
26.7 |
-10.3 |
412 |
17 |
29.3 |
-11 |
440 |
18 |
31.8 |
-12.1 |
484 |
19 |
34 |
-12.7 |
508 |
20 |
36.4 |
-13.8 |
552 |
20.5 |
37.6 |
-14.3 |
572 |
21 |
38.6 |
-14.6 |
584 |
21.5 |
40.1 |
-15.1 |
604 |
22 |
41.2 |
-15.55 |
622 |
22.5 |
42.3 |
-16 |
640 |
23 |
43.7 |
-16.8 |
672 |
LASER Documentation
PROBE safety documentation