1.3 mm probe X/Y/H-F H13863

Probe description: PH MASDVT 850W6 BL1.3 X/Y/H-F

Maximum spinning speed 65kHz

Additional components: shunt capacitor 220pF; shunt capacitor 180pF

x/y combination	X f/MHz	Y f/MHz	Modification mode	Description insert	Part no:
²⁹Si/¹⁵N-²H	168.9	86-130.5	λ/4	5 turns+ 1turn 12pF+3.3pF	HZ16604
¹³C/¹⁵N-²H	213.7	86 - 130.5	λ/4	4 turns+1 turn 8.2pF+3.3pF	HZ15355
²³Na/¹⁵N-²H	224.8	86 -130.5	λ/4	5 turns+ 1turn 6.8pF+3.3pF	HZ16606
²³Na/²⁹Si	224.8	168.9	λ/2	5 turns+ 1turn 6.8pF+3.3pF	HZ16606
²³Na/¹⁴N	224.8	61.4	with 220pF shunt and λ/4	5 turns+ 1turn 6.8pF+3.3pF	HZ16606
²⁷Al/¹⁴N-²⁹Si	221.5	61.4-168.9	the same modifications as ²³Na with 180pF for ¹⁴N	5 turns+ 1turn 6.8pF+3.3pF	HZ16605
¹¹B/¹⁷O-²⁹Si	272.7	115.2-168.9	λ/2	6 turns+ 1turn 3.3pF+3.3pF	HZ16607

Probe Test Results (Stated 90^o pulse lengths are the best achieved during installation. To reduce risk of damage to the probes, facility users should use slightly lower RF nutation frequencies (i.e. longer 90^o pulse lengths) were possible. Please discuss with the facility manager appropriate RF nutation frequencies for your experiments.)

insert ²⁹Si/¹⁵N-²H:

Nuc	90^opulse	Pulse power level (db)	Pulse power (W)	Configuration ²⁹Si/¹⁵N-²H	Sample	Remarks
²⁹Si	1.7	1	213	λ/4	Si-grease
¹⁵N	2	-1	442	λ/4	Glycine (CP)	S/N=5 (for 16 scans)
¹H	1.23	4	71	λ/4	Glycine	acquisition time tested 45ms

insert ¹³C/¹⁵N-²H:

Nuc	90^opulse	Pulse power level (db)	Pulse power (W)	Configuration ¹³C/¹⁵N-²H	Sample	Remarks
⁷⁹Br	1.5	3.3	136	λ/4	KBr
¹³C	1.5	3.3	142	λ/4	Adamantane	line width 1.6Hz
¹H	1	1.6	123	λ/4	Adamantane	there is a ¹H background visible
¹³C	2	5	96	λ/4	Glycine (CP)	S/N 42 (for 16 scans)
¹H	1.23	3.6	78	λ/4	Glycine	100kHz for 50ms decoupling
¹⁵N	3.45	-2	556	λ/4	Glycine (CP) (enriched)
¹⁹F	0.8	0	187	λ/4 for ¹⁹F	pvdf
¹⁹F	1.15	7	50	λ/4 for ¹⁹F	pvdf	there is a ¹⁹F background visible
¹³C	1.8	4	121	λ/4 for ¹⁹F	pvdf (¹⁹F CP)

insert ²³Na/¹⁵N-²⁹Si:

Nuc	90^opulse	Pulse power level (db)	Pulse power (W)	Configuration ²³Na/¹⁵N-²⁹Si	Sample	Remarks
²³Na	1.43	2	185	λ/4	NaCl
¹⁵N	2	-1	442	λ/4	Glycine (CP)
¹H	1.23	4	71	λ/4	Glycine
¹⁴N	2.3	0	398	λ/4	NH₄Cl

insert ²⁷Al/¹⁵N-²⁹Si:

Nuc	90^opulse	Pulse power level (db)	Pulse power (W)	Configuration ²⁷Al/¹⁵N-²⁹Si	Sample	Remarks
²⁷Al	1.6	2	156	λ/4	Al₂NO₃
¹⁵N	2	-1	442	λ/4	Glycine (CP)
¹H	1.23	4	71	λ/4	Glycine

insert ¹¹B/²⁹Si-¹⁷O:

Nuc	90^opulse	Pulse power level (db)	Pulse power (W)	Configuration ¹¹B/²⁹Si-¹⁷O	Sample	Remarks
¹¹B	1.15	3.3	116	λ/2	Borax
²H	2.3	0	232	λ/2	D₂O

DR mode:

Nuc	90^opulse	Pulse power level (db)	Pulse power (W)	Configuration	Sample	Remarks
¹³C	1.2	3.3	136	λ/2	Adamantane	line width 1.2Hz
¹H	.95	1.6	123	λ/2	Adamantane
¹³C	1.6	5	96	λ/2	Glycine (CP)	S/N 53 (16 scans)
¹H	1.27	3.8	74	λ/2	Glycine
¹⁹F	0.82	4.3	93	λ/4	pvdf
¹³C	1.25	3.3	136	λ/4	pvdf

Tuning ranges (tested on the bench; probe in double-resonance mode ¹H-X)

λ /4 mode	61 →132 MHz	Includes: ¹⁴N(61.424), ³³S(65.246), ¹⁸⁹Os(66.006), ²¹Ne(67.102), ¹⁷⁶Lu(69.114), ³⁷Cl(69.324), ¹³¹Xe(70.073), ¹⁶⁹Tm(70.465), ⁶¹Ni(75.956), ⁹¹Zr(79.019), ⁸⁵Rb( 82.067), ³⁵Cl (83.282), ¹³⁵Ba( 84.443), ⁵⁰V( 84.748), ¹⁵N( 86.163), ¹⁰B(91.321), ¹⁵³Eu(93.330), ¹³⁷Ba( 94.460), ¹⁷⁵Lu( 96.934), ¹⁸¹Ta(101.912), ¹²³Sb( 110.153), ¹³³Cs(111.487), ¹³⁸La(112.152), ¹⁷O(115.230), ⁹Be( 119.440), ¹³⁹La(120.068), ⁶Li(125.087), ²H(130.480)
λ/2 mode	150 → 215 MHz	Includes: ⁷⁷Se(162.108), ²⁹Si(168.871), ¹²⁷I(170.064), ²⁰⁷Pb( 177.825), ¹¹¹Cd(180.332), ¹⁶⁵Ho(181.390), ¹⁹⁵Pt(182.723), ¹¹³In(185.859), ¹¹⁵In(186.257), ¹¹³Cd(188.642), ⁹⁹Tc(191.321), ¹⁸⁵Re(191.459), ¹⁸⁷Re(193.389), ⁵⁹Co(201.680), ¹²¹Sb(203.410), ⁶⁹Ga(204.012), ¹⁵⁹Tb(204.340), ⁴⁵Sc(206.480), ⁹³Nb(208.047), ⁵⁵Mn(210.708), ¹⁵¹Eu(211.310), ⁷⁹Br(212.959), ¹³C(213.733)
λ/2 mode + range coil	220 → 280 MHz	²⁷Al (221.483), ¹²³Te(222.443), ⁵¹V(223.575), ²³Na(224.841), ⁶³Cu(225.382), ⁸¹Br(229.555), ¹²⁹Xe(236.387), ⁶⁵Cu(241.431), ⁷¹Ga(259.222), ¹⁴¹Pr(260.270), ¹²⁵Te(268.173), ¹¹B(272.714), ¹¹⁵Sn(278.109), ⁸⁷Rb(278.124), ¹¹⁷Sn(302.874), ¹¹⁹Sn(316.970), ⁷Li(330.342), ³¹P(344.086)